An Elegant Microwave Assisted One-Pot Synthesis of Di(alpha-aminophosphonate) Pesticides

作者:Reddy Gangireddy Chandra Sekhar; Rani Chinthaparthi Radha; Reddy Mudumala Veera Narayana; Reddy Cirandur Suresh*
来源:Archiv der Pharmazie, 2014, 347(11): 819-824.
DOI:10.1002/ardp.201400213

摘要

A new class of di(-aminophosphonate) pesticides were prepared by the Kabachnik-Fields reaction under solvent- and catalyst-free conditions with microwave irradiation, and the products were obtained in good-to-excellent yields at shorter reaction time. These compounds were characterized by IR, H-1, C-13, P-31 NMR, and mass spectral data. Among them, compounds 4f, 4c, and 4h showed good pesticidal activity against Spodoptera litura, with 92.6, 91.3, and 89.3% mortality.

  • 出版日期2014-11