科研之友
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摘要
A simple chemical synthetic route has been developed to prepare nanocrystalline titanium nitride (TiN) in an autoclave, by the reaction of metallic Ti with NaNH(2) at low temperature of 500-600 degrees C. The samples were characterized by X-ray powder diffraction, transmission electron microscopy, and X-ray photoelectron spectra. The possible reaction mechanism of this process is also discussed. This method may be extended to the synthesis of other metal nitrides.
- 出版日期2011
- 单位中国矿业大学（北京）
