Microwave absorption study of carbon nano tubes dispersed hard/soft ferrite nanocomposite

作者：Tyagi Sachin^*; Verma Palash; Baskey Himanshu B; Agarwala Ramesh Chandra; Agarwala Vijaya; Shami Trilok Chand

来源：Ceramics International, 2012, 38(6): 4561-4571.

DOI：10.1016/j.ceramint.2012.02.034

• Sol-gel processes
• Composites
• Dielectric properties

Nickel substituted strontium hexaferrite, SrNi2Fe10O19 center dot(SrFe12O19/NiFe2O4) nanoparticles have been synthesized by low combustion method by citrate precursors using sal to gel (S-G) followed by gel to nano crystalline (G-N) conversion. The resulting 'as-synthesized' powder is heat treated (HT) at 800 and 1000 degrees C for 4 h in nitrogen atmosphere. The hysteresis loops show an increase in saturation magnetization from 27.443 to 63.706 emu/g with increasing HT temperatures. The multiwalled carbon nano tubes (CNTs) were synthesized by thermal decomposition of acetylene gas over iron-catalyst deposited on silicon wafer in the temperature range of 750-800 degrees C. A microwave absorbing medium is prepared by adding CNTs in the nickel substituted stronitum hexaferrite nanoparticles. Addition of certain mass of CNTs improves the microwave absorption properties and wave band of SrFe12O19/NiFe2O4 absorbent. When 10 wt% CNTs is mixed with SrFe12O19/NiFe2O4 nanoparticles to fabricate a composite with 2 mm thickness, the maximum reflection loss reaches to -36.817 dB at 9.292 GHz and -10 dB bandwidth reaches 3.27 GHz.

• 出版日期2012-8