A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates

作者：Berestovitskaya Valentina M^*; Ozerova Olga Yu; Efimova Tatiana P; Gurzhiy Vladislav V; Novikova Tamara A

来源：Mendeleev Communications, 2016, 26(4): 323-325.

DOI：10.1016/j.mencom.2016.07.019

Reaction of 1-amino-2-nitroguanidine with alkyl 3-bromo-3-nitropropenoates affords 3-nitrohnino-6-nitromethyl-4,5-dihydro-(2H)-1,2,4-triazin-5-one, whose structure was characterized by IR, UV, NMR spectroscopy and X-ray single crystal analysis.

• 出版日期2016-8