Grain boundary segregation of minor arsenic and nitrogen at elevated temperatures in a microalloyed steel

作者：Zhu, Yuan-zhi^*; Zhu, Zhe; Xu, Jian-ping

来源：International Journal of Minerals Metallurgy and Materials, 2012, 19(5): 399-403.

DOI：10.1007/s12613-012-0570-x

• alloy steel
• arsenic
• nitrogen
• segregation
• grain boundaries

Auger electron spectroscopy (AES) was used to investigate the grain boundary segregation of arsenic and nitrogen in a kind of microalloyed steel produced by a compact strip production (CSP) technology at 950 to 1100 degrees C, which are similar to the hot working temperature of the steel on a CSP production line. It was discovered that arsenic segregated on grain boundaries when the steel was annealed at 950 degrees C for 2 h. When the annealing temperature increased to 1100 degrees C, arsenic was also found to have segregated on grain boundaries in the early annealing stage, for instance, within the first 5 min annealing time. However, if the holding time of the steel at this temperature increased to 2 h, arsenic diffused away from grain boundaries into the matrix again. Nitrogen was not found to have segregated on grain boundaries when the steel was annealed at a relatively low temperature, such as 950 degrees C. But when the annealing temperature increased to 1100 degrees C, nitrogen was detected to have segregated at grain boundaries in the steel.

• 出版日期2012-5
• 单位武汉科技大学