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摘要
The new three-dimensional coordination polymer {[Bi(NNO)(2)(NO3)]center dot 1.5H(2)O}(n) (1, NNO = nicotinate N-oxide) was synthesized and characterized by elemental analysis, IR and H-1-NMR spectroscopy, as well as single-crystal X-ray diffraction analysis. 1 crystallizes in the monoclinic space group C2/c. The crystal structure consists of a rectangular-shaped grid constructed with NNO linkers. Cavities of a diameter of 7.9-8.3 angstrom(2) are filled with disordered water molecules. The thermal stability of the compound was evaluated by thermogravimetric analysis.
- 出版日期2013
