A simple route to prepare nanocrystalline titanium carbonitride

作者：Shen GZ; Tang KB^*; An CH; Yang Q; Wang CR; Qian YT

来源：Materials Research Bulletin, 2002, 37(6): 1207-1211.

DOI：10.1016/S0025-5408(02)00736-5

• nanostructures
• chemical synthesis
• X-ray diffraction

Nanocrystalline titanium carbonitride, TiC0.7N0.3, has been synthesized directly by a simple reaction route of TiCl4 and C3N3Cl3 using sodium as the reductant at 600degreesC. The composition of the powders has been investigated by X-ray powder diffraction. Transmission electron microscopy image reveals that the average size of the obtained particles is about 30 nm.

• 出版日期2002-5
• 单位中国科学技术大学