Magic-angle-spinning NMR at 30 T with a hybrid magnet

作者：Hashi Kenjiro^*; Shimizu Tadashi; Fujito Teruaki; Goto Atsushi; Ohki Shinobu; Shimoda Keiji; Tobu Yasuhiro; Saito Koji

来源：Chemistry Letters, 2007, 36(7): 884-885.

DOI：10.1246/cl.2007.884

Solid-state NMR measurements at 30T have been performed with a hybrid magnet of National Institute for Materials Science. Spectral resolution less than 3 ppm was confirmed by Br-79 magic-angle-spinning (MAS)NMR measurements of a reference material KBr. A small sample and an aluminum metal shield were used to reduce the effects of field inhomogeneity and fluctuation. As an example of application for an industrial material, Al-27 MAS NMR of a refractory mortar was demonstrated.

• 出版日期2007-7-5