Design of a portable gas chromatography with a conducting polymer nanocomposite detector device and a method to analyze a gas mixture

作者：Pirsa Sajad^*

来源：Journal of Separation Science, 2017, 40(8): 1724-1730.

DOI：10.1002/jssc.201601393

• amines
• conducting polymer
• nanocomposite
• portable system
• simultaneous determination

A portable chromatography device and a method were developed to analyze a gas mixture. The device comprises a chromatographic column for separating components of a sample of the gas mixture. It has an air pump coupled to the inlet of a chromatographic column for pumping air and an injector coupled to the inlet of chromatographic column for feeding the sample using the air as a carrier gas. A detector is arranged downstream from and coupled to the outlet of the chromatographic column. The detector is a nanostructure semiconductive microfiber. The device further comprises an evaluation unit arranged and configured to evaluate each detected component to determine the concentration. The designed portable system was used for simultaneous detection of amines. The possibility of applying dispersive liquid-liquid microextraction for the determination of analytes in trace levels is demonstrated. The reproducibility of this method is acceptable, and good standard deviations were obtained. The relative standard deviation value is less than 6% for all analytes. Finally, the method was successfully applied to the extraction and determination of analytes in water samples.

• 出版日期2017-4