Ammonium Oxalate as an Efficient Catalyst for One-Pot Synthesis of Tetrahydrobenzo [a]xanthen-11-one Derivatives Under Solvent-Free Conditions

作者:Esfahani Hamid R M; Foroughifar Naser*; Mobinikhaledi Akbar; Moghanian Hassan
来源:Synthesis and Reactivity in Inorganic Metal-Organic and Nano-Metal Chemistry, 2013, 43(6): 752-755.
DOI:10.1080/15533174.2012.754767

摘要

A simple and efficient procedure for the synthesis of 12-aryl- or 12-alkyl-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one derivatives has been developed via one-pot three-component reaction of 2-naphthol, aldehydes, and dimedone in the presence of ammonium oxalate as a mild and inexpensive catalyst under solvent-free conditions. The present method is operationally simple and offers several advantages such as high yields, short reaction time, economic availability of the catalyst, and simple workup.

  • 出版日期2013-7-3

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