Microwave-assisted polyol synthesis of nanoscale SnSx(x=1,2) flakes

作者:Chen D; Shen GZ; Tang KB*; Lei SJ; Zheng HG; Qian YT
来源:Journal of Crystal Growth, 2004, 260(3-4): 469-474.
DOI:10.1016/j.jcrysgro.2003.09.009

摘要

The tin sulfides compounds SnS and SnS2 nanoflakes were prepared by the microwave-assisted polyol synthetic method. The as-prepared nanoscale flakes were characterized by X-ray powder diffraction, transmission electron microscopy, selected area electron diffraction, X-ray photoelectron spectroscopy and Raman spectra. The influences of solvents and microwave irradiation on the formation of products have been studied.