Achievement of H-1-F-19 heteronuclear experiments using the conventional spectrometer with a shared single high band amplifier

作者：Sakuma Chiseko; Kurita Jun ichi; Furihata Kazuo; Tashiro Mitsuru^*

来源：Magnetic Resonance in Chemistry, 2015, 53(5): 327-329.

DOI：10.1002/mrc.4210

• F-19 NMR
• H-1-F-19 heteronuclear experiments
• conventional spectrometer
• F-19{H-1} and H-1{F-19} STD

The H-1-F-19 heteronuclear NMR experiments were achieved using the conventional spectrometer equipped with a single high band amplifier and a H-1/F-19/C-13 double-tuned probe. Although double high band amplifiers are generally required to perform such experiments, a simple modification of pathway in the conventional spectrometer was capable of acquiring various H-1-F-19 heteronuclear spectra. The efficiency of the present technique was demonstrated in an application for F-19{H-1} and H-1{F-19} saturation transfer difference experiments.

• 出版日期2015-5