科研之友
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摘要
Reactions of molybdenum and chromium hexacarbonyls with isatin-3-oxime (H2L) in THF were carried out under sun light or according to the traditional thermal reflux synthetic routes. Di-mu-oxo bimolybdenum complex, [Mo(H2L)(THF)(O)(2)](2) was successfully synthesized under the reflux conditions. However, the dichromium oxo complex, [Cr(H2L)(P)(2)](2) was prepared using the sun light route. The prepared complexes were characterized using elemental analysis, IR, mass spectrometry, UV-Vis spectra, thermal analysis, and magnetic measurements.
- 出版日期2012-10-24
