Hydrothennal synthesis and characterization of nanocrystalline PZT powders

作者：Deng Y; Liu L; Cheng Y; Nan CW^*; Zhao SJ

来源：Materials Letters, 2003, 57(11): 1675-1678.

DOI：10.1016/S0167-577X(02)01050-9

• PZT
• nanostructures
• hydrothermal synthesis

In this paper, nano-sized lead zirconate-titanate (PZT) powders were synthesized without using any excess lead content by a hydrothermal method based on the reaction of TiO2, Pb(NO3)(2), ZrOCl2.8H(2)O or Zr(NO3)(4).5H(2)O and KOH at 160 degreesC for 4 h. The powders were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The PZT powder consists of nearly homogenous and spherical grains with an average diameter of 5-10 nm. A possible formation mechanism is proposed.

• 出版日期2003-3
• 单位清华大学; 佳木斯大学