Preparation of Ni-MCM-41 by electroless plating

作者：Chen Jian; Zhang Guangxu^*; Gao Weifang; Fang Yuan; Shu Ting; Cai Weiquan

来源：Journal of the Chinese Ceramic Society, 2014, 42(7): 903-907.

DOI：10.7521/j.issn.0454-5648.2014.07.15

• Adsorption desorption
• Analysis techniques
• Electroless nickel-plating
• Metallic composites
• Ni-MCM-41
• Optimal temperature
• Potential hydrogens
• Ultrosonic method

The nickeliferous MCM-41 is one of potential hydrogen storage materials with excellent properties. MCM-41 was synthesized by hydrothermal synthesis method, and then electroless plating was employed to deposit Ni on the surface of MCM-41 under the mixing pattern of mechanical stir and ultrasonic to prepare Ni-MCM-41. The prepared samples were characterized by X-ray powder diffraction, transmission electron microscopy and N2adsorption-desorption analysis techniques. The results showed that this method is feasible, and had a good effect on the structure of MCM-41. Ultrasonic way benefited the effect of plating, and the optimal temperature was 80°C. It means that electroless plating is a good candidate for preparing metal-containing mesoporous materials.

• 出版日期2014
• 单位武汉理工大学