摘要

Nickel molybdate nanosheets were synthesized by a microwave-assisted solvothermal method, and the structure and morphology of the as-prepared nanosheets were characterized by powder X-ray diffraction (PXRD), transmission electron microscope (TEM), and high-resolution TEM (HRTEM). Serving as a non-enzymatic sensor, the NiMoO4 nanosheet modified carbon paste electrode (CPE) demonstrated excellent electrocatalytic activity towards glucose oxidation with a high sensitivity and good stability. The results suggest that the NiMoO4 nanosheet is a promising electrode material for enzyme-free glucose sensors.