N'-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvate

作者:Han Ling; Huang Shan Shan; Huang Qing Bai; Zhou Xue Mei; Diao Yun Peng*
来源:Acta Crystallographica Section E-Structure Reports Online, 2008, 64(5): O781-U1220.
DOI:10.1107/S160053680800843X

摘要

The title compound, C14H10ClN3O4 center dot CH4O, was synthesized from the reaction of 5-chlorosalicylaldehyde with 4-nitrobenzohydrazide in methanol. The Schiff base molecule is nearly planar, with a dihedral angle of 9.1 (3)degrees between the two benzene rings. The methanol solvent molecules are linked to the Schiff base molecules by N-H center dot center dot center dot O, O-H center dot center dot center dot N and O-H center dot center dot center dot O hydrogen bonds, forming chains running parallel to the a axis.