Ultrafast Synthesis of LTA Nanozeolite Using a Two-Phase Segmented Fluidic Microreactor

作者：Zhou, Jianhai; Jiang, Hao; Xu, Jian; Hu, Jun^*; Liu, Honglai; Hu, Ying

来源：Journal of Nanoscience and Nanotechnology, 2013, 13(8): 5736-5743.

DOI：10.1166/jnn.2013.7555

• Microfluidic Reactor
• LTA Zeolite
• Ultrafast Synthesis
• Nanostructures

Fast synthesis of nanosized zeolite is desirable for many industrial applications. An ultrafast synthesis of LTA nanozeolite by the organic-additive-free method in a two-phase segmented fluidic nnicroreactor has been realized. The results reveal that the obtained LTA nanozeolites through microreactor are much smaller and higher crystallinity than those under similar conditions through conventional macroscale batch reactor. By investing various test conditions, such as the crystallization temperature, the flow rate, the microchannel length, and the aging time of gel solution, this two-phase segmented fluidic microreactor system enables us to develop an ultrafast method for nanozeolite production. Particularly, when using a nnicroreactor with the microchannel length of 20 m, it only takes 10 min for the crystallization and no aging process to successfully produce the crystalline LTA nanozeolites at 95 degrees C.

• 出版日期2013-8
• 单位华东理工大学; 上海市计量测试技术研究院