Stepwise injection photometric determination of nickel in air aerosols

作者:Bulatov A V*; Fulmes K S; Moskvin A L; Moskvin L N
来源:Journal of Analytical Chemistry, 2013, 68(1): 68-71.
DOI:10.1134/S1061934813010048

摘要

A procedure is developed for the automated determination of nickel in air aerosols; it involves the adhesive separation of aerosols on a fiberglass column in the on-site mode followed by the photometric determination of analytes with dimethyl glyoxime under the conditions of stepwise injection analysis of aerosol concentrates. The analytical range for nickel is 1.5-38 mu g/m(3); the detection limit of the method is 0.5 mu g/m(3) at an air sample volume of 30 L. The duration of sampling to an adhesive column and concentrate analysis were 15 and 10 min, respectively.

  • 出版日期2013-1

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