科研之友
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摘要
The selective reduction of nitro compounds by treatment with bimetallic Fe-Ni nanoparticles (NPs) and tungestophosphoric acid hydrate (H3PW12O4o.xH(2)O) in H2O is reported. The method has been applied to a broad range of nitro compounds with different sensitive functionalities, including halides, carbonyl, hydroxyl, aldehyde, methyl, acetyl, nitrile, and ester substituents with excellent yields. The reaction yielded single product in all cases with very high yield. The simple experimental procedure and easy purification make the protocol advantageous.
- 出版日期2014-10
