Ultrafast hydrothermal synthesis of Pr-doped Ca0.6Sr0.4TiO3 red phosphor nanoparticles using corrosion resistant microfluidic devices with Ti-lined structure under high-temperature and high-pressure condition

作者：Sue Kiwamu^*; Ono Takeshi; Hakuta Yukiya; Takashima Hiroshi; Nishio Hamane Daisuke; Sato Takafumi; Ohara Motohiro; Aoki Mitsuko; Takebayashi Yoshihiro; Yoda Satoshi; Hiaki Toshihiko; Furuya Takeshi

来源：Chemical Engineering Journal, 2014, 239: 360-363.

DOI：10.1016/j.cej.2013.11.035

• Microfluidic device
• Hydrothermal synthesis
• Red phosphor
• Oxide nanoparticles
• High temperature
• Corrosion resistance

Corrosion resistant microfluidic devices with Ti-lined structure were fabricated for hydrothermal synthesis of high purity metal oxide nanoparticles under high-temperature and high-pressure condition. Pr-doped Ca0.6Sr0.4TiO3 red phosphor nanoparticles without contaminations were continuously and safely synthesized using the devices at 673 K and 30 MPa within short residence time of 20 ms in spite of corrosive environment. The nanoparticles having an average particle size of 10 nm and a perovskite structure showed a strong red emission peak around 613 nm.

• 出版日期2014-3-1