Developments and applications of capillary microextraction techniques: A review

作者：Kataoka Hiroyuki^*; Ishizaki Atsushi; Nonaka Yuko; Saito Keita

来源：Analytica Chimica Acta, 2009, 655(1-2): 8-29.

DOI：10.1016/j.aca.2009.09.032

• Sample preparation
• Capillary microextraction
• Open-tubular trapping
• In-tube solid-phase microextraction
• On-line analysis
• Automated analysis

Sample preparation is important for isolating desired components from complex matrices and greatly influences their reliable and accurate analysis. Recent trends in sample preparation include miniaturization, automation, high-throughput performance, and reduction in solvent consumption and operation time. This review focuses on novel microextraction techniques using capillaries for off-line and on-line sample preparation. Open-tubular trapping (OTT), in-tube solid-phase microextraction (SPME), wire-in-tube SPME, fiber-in-tube solid-phase extraction (SPE), sorbent-packed capillary in-tube SPME and monolithic capillary in-tube SPME are critically evaluated and applications of these techniques in biological, pharmaceutical, environmental and food analyses are summarized.

• 出版日期2009-11-23