Mass-spectrometric investigations of the synthesis of silver nanoparticles via electrolysis

作者：Szymanska Chargot M; Gruszecka A; Smolira A; Cytawa J; Michalak L^*

来源：Vacuum, 2008, 82(10): 1088-1093.

DOI：10.1016/j.vacuum.2008.01.022

• silver nanoparticles
• electrolysis
• laser desorption
• TOFspectrometer

The synthesis of silver nanoparticles during electrolysis of NaCl solutions and silver electrodes was controlled by using UV absorption and mass-spectrometric methods. For mass-spectrometric measurements, the laser desorption/ionization method and a time of flight (TOF) spectrometer were employed. Results of investigations show the possibility of formation of small silver nanoparticles (of the cluster size <= 7) or their compounds.

• 出版日期2008-6-3