Development of a combined portable x-ray fluorescence and Raman spectrometer for in situ analysis

作者：Guerra M^*; Longelin S; Pessanha S; Manso M; Carvalho M L

来源：Review of Scientific Instruments, 2014, 85(6): 063113.

DOI：10.1063/1.4883188

In this work, we have built a portable X-ray fluorescence (XRF) spectrometer in a planar configuration coupled to a Raman head and a digital optical microscope, for in situ analysis. Several geometries for the XRF apparatus and digital microscope are possible in order to overcome spatial constraints and provide better measurement conditions. With this combined spectrometer, we are now able to perform XRF and Raman measurements in the same point without the need for sample collection, which can be crucial when dealing with cultural heritage objects, as well as forensic analysis. We show the capabilities of the spectrometer by measuring several standard reference materials, as well as other samples usually encountered in cultural heritage, geological, as well as biomedical studies.

• 出版日期2014-6