Fast and efficient synthesis of 10-aryl-2,7-dimethyl-4,5-dioxo-3,6,9-trioxa-3,4,5,6,9,10-hexahydroanthra cene under microwave irradiation without catalyst

作者：Gao Yuan; Tu Shujiang^*; Shi Feng; Wang Qian; Zhu Xiaotong; Shi Daqing

来源：Synthetic Communications, 2007, 37(10): 1603-1608.

DOI：10.1080/00397910701263601

• aromatic aldehyde
• microwave irradiation
• triacetic acid
• trioxanthene

A fast and efficient synthetic method for the title compounds is described. By heating aromatic aldehyde and triacetic acid lactone in ethylene glycol under microwave irradiation without catalyst for 3-5 min, 10-aryl- 2,7-dimethyl- 4,5-dioxo3,6,9- trioxa-3,4,5,6,9,10-hexahydroanthracenes were afforded with high yields.

• 出版日期2007
• 单位江苏师范大学