Fabrication and mechanical properties of Al2O3-SiCw-TiCnp ceramic tool material

作者：Zhao, Bin; Liu, Hanlian^*; Huang, Chuanzhen; Wang, Jun^*; Cheng, Moli

来源：Ceramics International, 2017, 43(13): 10224-10230.

DOI：10.1016/j.ceramint.2017.05.049

• Ceramic tool material
• SiC whisker
• TiC nanoparticle
• Particle size
• Mechanical properties

Whiskers and nanoparticles are usually used as reinforcing additives of ceramic composite materials due to the synergistically toughening and strengthening mechanisms. In this paper, the effects of TiC nanoparticle content, particle size and preparation process on the mechanical properties of hot pressed Al2O3-SiCw ceramic tool materials were investigated. The results showed that the Vickers hardness and fracture toughness of the materials increased with the increasing of TiC content. The optimized flexural strength was obtained with TiC content of 4 vol% and particle size of 40 nm. The particle size has been found to have a great influence on flexural strength and small influence on hardness and fracture toughness. It was concluded that the flexural strength increased remarkably with the decreasing of the TiC particle size, which was resulted from the improved density and refined grain size of the composite material due to the dispersion of the smaller TIC particle size. SEM micrographs of fracture surface showed the whiskers to be mainly distributed along the direction perpendicular to the hot-pressing direction. The fracture toughness was improved by whisker crack bridging, crack deflection and whisker pullout; the TiC nanoparticles in Al2O3 grains caused transgranular fracture and crack deflection, which improved the flexural strength and fracture toughness with whiskers synergistically. Uniaxial hot-pressing of SiC whisker reinforced Al2O3 ceramic composites resulted in the anisotropy of whiskers' distribution, which led to crack propagation differences between lateral crack and radical crack.

• 出版日期2017-9
• 单位山东大学