Mechanochemical route for sulphide nanoparticles preparation

作者:Balaz P*; Boldizarova E; Godocikova E; Briacin J
来源:Materials Letters, 2003, 57(9-10): 1585-1589.
DOI:10.1016/S0167-577X(02)01037-6

摘要

Well-crystallized ZnS, US and PbS nanoparticles were successfully synthesized by the mechanochemical route from the corresponding acetates and Na2S. X-ray powder diffraction and scanning electron microscopy were used to characterize the as-obtained products. The SEM measurements show the aggregates of small nanocrystals in which particle sizes of 5-18 nm. were estimated by Scherrer's formula. Simple flow chart of the preparation of sulphide nanoparticles was presented.

  • 出版日期2003-2