科研之友
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摘要
Here, we report the development of a simple, small, fast heating, and portable, homemade, inert gas (Ar) atmospheric annealing setup. Instead of using a conventional heating element, a commercial soldering rod having an encapsulated fast heating heater is used here. The sample holder is made of a block of stainless steel. It takes 200 s to reach 700 degrees C, and 10 min to cool down. The probability of oxidation or surface contamination has been examined by means of x ray photoelectron spectroscopy of virgin Cu sample after annealing at 600 degrees C. In addition, we compare the annealing of a hydrogenated carbon nitride film (HCNx) in both a conventional vacuum and our newly developed ambient Ar atmosphere setup.
- 出版日期2012-4
