Mechanical properties and microstructure of 3D orthogonal quartz fiber reinforced silica composites fabricated by silicasol-infiltration-sintering

作者：Li, Chengdong; Chen, Zhaofeng; Zhu, Jianxun^*; Liu, Yong; Jiang, Yun; Guan, Tianru; Li, Binbin; Lin, Long

来源：Materials & Design, 2012, 36: 289-295.

DOI：10.1016/j.matdes.2011.11.022

• Ceramic matrix composites
• Mechanical
• Microstructure

3D orthogonal quartz fiber reinforced silica composites were fabricated by silicasol-infiltration-sintering method at a low temperature of 450 degrees C, and the mechanical properties and microstructure of the composites were investigated. The density of the composites was 1.71 g/cm(3), the average values of flexure strength and shear strength of the composites were 29.4 MPa and 14.8 MPa at room temperature, respectively. Both of the failures under flexural loading and shear loading were not catastrophic. Compared with alpha-quartz and alpha-cristobalite, the fracture toughness of 3D orthogonal quartz fiber reinforced silica composites has been enhanced by a wide margin. The damage features of the composites are identified, using digital camera and scanning electron microscopy. There was a good state without serious degradation of quartz fibers during the preparation. The bonding between the matrix and the incorporated fibers is weak, and the matrix cracks propagate along the weak interface. Apart from this, the composite is found to exhibit an extensive and long fiber pull-out in the fracture surface. Crack deflection and fiber pull-out contributed to the good toughness of the composite under the loading.

• 出版日期2012-4
• 单位中材科技股份有限公司; 南京航空航天大学