Novel application of nanocrystalline nickel electrodeposit: Making good diamond tools easily, efficiently and economically

作者：Li Yundong^*; Jiang Hui; Pang Lijuan; Wang Bao'an; Liang Xiaohui

来源：Surface and Coatings Technology, 2007, 201(12): 5925-5930.

DOI：10.1016/j.surfcoat.2006.10.047

• vickers hardness test
• electroplating
• nickel
• nanostructure
• electroplated diamond tools

Electrodeposition has been identified as a feasible and economical technique for nanomaterials application. This article details an improved approach to producing better diamond tools at lower cost and with higher productivity. Pulse-electroformed nanocrystalline nickel was used as the new matrix. The pulse parameters were determined after examination of the microstructure, grain size, hardness and tensile strength of the deposits obtained at different average current densities (J(m)) with constant pulse-on time and pulse-off time. It is shown that, with J(m) ranging from 1 Adm(-2) 2 to 14 Adm(-2), the grain size decreases sharply from 180 nm to about 10 nm while the hardness and tensile strength significantly increase at first and then reach their peaks respectively, although the strength fails to stay long. Current density J(m) that produced the highest hardness and strength of deposit (with grain size of 20 nm) was chosen for new diamond tools that exhibited 20.2% longer service life than their usual Ni-Co counterparts. Therefore, nanocrystalline electrodeposits are expected to be an upgrading substitute for conventional polycrystalline matrix.

• 出版日期2007-3-5
• 单位河南农业大学