An easy purification of glycoluril clips by affinity chromatography

作者:Golari Neda; Rahimizadeh Mohammad; Bakavoli Mehdi; Rezaei Seresht Esmail*
来源:Journal of Inclusion Phenomena and Macrocyclic Chemistry, 2014, 80(3-4): 353-358.
DOI:10.1007/s10847-014-0414-6

摘要

A convenient method for separation and purification of glycoluril clips was developed on the basis of affinity chromatography using a resorcinol-functionalized Merrifield resin. The modified resin was readily prepared via immobilization of phlroglucinol on Merrifield resin. It was used for successful isolation of the desired clip products from their corresponding reaction mixtures. Also, the resin could be repeatedly recycled and reused without any noticeable decrease in its effectiveness.

  • 出版日期2014-12