Diethylamine-Catalyzed Dimerization of Thiols: An Inexpensive and Green Method for the Synthesis of Homodisulfides Under Aqueous Conditions

作者：Abaee M Saeed^*; Mojtahedi Mohammad M; Navidipoor Somayeh

来源：Synthetic Communications, 2011, 41(2): 170-176.

DOI：10.1080/00397910903531904

• Aqueous conditions
• disulfides
• oxidation
• thiols

Under H2O / Et2NH / atmospheric oxygen conditions, thiols are converted to their respective homodisulfides within a few hours. The process is conducted at room temperature for quantitative dimerization of aromatic, benzylic, and aliphatic thiols without the use of any extra additive.

• 出版日期2011