Determination of Dry Matter Content in Potato Tubers by Low-Field Nuclear Magnetic Resonance (LF-NMR)

作者:Hansen Christian Lyndgaard*; Thybo Anette Kistrup; Bertram Hanne Christine; Viereck Nanna; van den Erg Frans; Engelsen Soren Balling
来源:Journal of Agricultural and Food Chemistry, 2010, 58(19): 10300-10304.
DOI:10.1021/jf101319q

摘要

The objective of this study was to develop a calibration model between time-domain low-field nuclear magnetic resonance (LF-NMR) measurements and dry matter (DM) content in single potatoes. An extensive sampling procedure was used to collect 210 potatoes from eight cultivars with a wide range in DM content, ranging from 16 to 28%. The exponential NMR relaxation curves were resolved into four mono-exponential components using a number of solution diagnostics. Partial least-squares (PLS) regression between NMR parameters (relaxation time constants T(2,1-4) and magnitudes M(0,1-4)) and DM content resulted in a model with low error (RMSECV, 0.71; RMSEP, 0.60) and high correlation (r(cv), 0.97; r(test), 0.98) between predicted and actual DM content. Correlation between DM content and each of the proton populations revealed that M0,1 (T(2,1), 3.6 ms; SD, 0.3 ms; r, 0.95) and M(0.4) (T(2,4), 508 ms; SD, 53 ms; r, -0.90) were the major contributors to the PLS regression model.

  • 出版日期2010-10-13