Photocrystallography - design and methodology for the use of a light-emitting diode device

作者:Brayshaw Simon K; Knight Jason W; Raithby Paul R*; Savarese Teresa L; Schiffers Stefanie; Teat Simon J; Warren John E; Warren Mark R
来源:Journal of Applied Crystallography, 2010, 43: 337-340.
DOI:10.1107/S0021889810004759

摘要

With the increase in interest in photocrystallographic experiments, the use of light-emitting diodes (LEDs) provides an alternative, low-budget light source (by comparison to lasers) and allows photocrystallographic experiments to be carried out readily. Here the design of an LED array device suitable for use in single-crystal X-ray diffraction experiments is reported, and the experimental methodology used for determining the structures of metastable species is described.

  • 出版日期2010-4