Hydrocarbon impurities in SiF4 and SiH4 prepared from it

作者:Bulanov A D*; Sennikov P G; Krylov V A; Sorochkina T G; Chuprov L A; Chernova O Yu; Troshin O Yu
来源:Inorganic Materials, 2007, 43(4): 364-368.
DOI:10.1134/S0020168507040061

摘要

Using gas chromatography and high-resolution Fourier-transform IR spectroscopy, we have determined the concentrations of C-1-C-4 hydrocarbon impurities in isotopically unmodified silicon tetrafluoride before and after fine purification and in Si-28-enriched SiF4. The concentrations of C-1-C-4 hydrocarbon impurities in silicon tetrafluoride for SiH4 synthesis have been shown to correlate with those in the synthesized silane.

  • 出版日期2007-4