A simple aqueous solution based chemical methodology for synthesis of Ag nanoparticles dispersed on mesoporous silicate matrix

作者：Naik Bhanudas; Prasad V S; Ghosh Narendra Nath^*

来源：Powder Technology, 2010, 199(2): 197-201.

DOI：10.1016/j.powtec.2010.01.005

• SBA-15
• Ag nanoparticle
• N(2) adsorption-desorption isotherm
• Mesoporous
• BET surface area

A simple chemical method has been developed for preparation of Ag nanoparticles dispersed on mesoporous silicate matrix, SBA-15. Ag nanoparticles were uniformly dispersed on SBA-15 matrix by using the reduction reaction of AgNO(3) with trisodium citrate. The synthesized materials were characterized by using room temperature powder XRD analysis, N(2) adsorption-desorption isotherm, high resolution TEM and SEM. It was observed that the synthesized SBA-15 and Ag-SBA-15 have a surface area of 778 and 151 m(2)/g respectively. The synthesized materials have long range ordering of pores with narrow pore size distribution centered at similar to 7 nm. Pore structure of SBA-15 remains preserved even after deposition of Ag nanoparticle. This chemical route reported here offers a simple method for preparation of Ag-SBA-15, where unagglomerated Ag nanoparticles (similar to 20 nm) are uniformly dispersed on SBA-15.

• 出版日期2010-4-23