Azines from one-pot reaction of thiosemicarbazones

作者:Aly Ashraf A*; Hassan Alaa A; Brown Alan B; Ibrahim Mahmoud A A; AbdAl Latif El Shimaa S M
来源:Journal of Sulfur Chemistry, 2017, 38(1): 11-17.
DOI:10.1080/17415993.2016.1210146

摘要

Thermolysis and/or microwave irradiation of thiosemicarbazones gave the corresponding isothiocyanates, which on addition of either activated nitriles or aldehydes furnished various types of azines. The mechanism was discussed. The structures of products were proved by MS, IR, NMR, and elemental analyses. [GRAPHICS]

  • 出版日期2017-2

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