Microflow photochemistry-a reactor comparison study using the photochemical synthesis of terebic acid as a model reaction

作者:Aida Shin; Terao Kimitada; Nishiyama Yasuhiro; Kakiuchi Kiyomi; Oelgemoeller Michael
来源:Tetrahedron Letters, 2012, 53(42): 5578-5581.
DOI:10.1016/j.tetlet.2012.07.143

摘要

The continuous-microflow photochemical synthesis of terebic acid from maleic acid was investigated in two different microreactor set-ups. The results were subsequently compared to analogue experiments in a conventional chamber reactor. Based on conversion rates, reactor design and energy efficiency calculations, the simple microcapillary reactor showed the best overall performance.

  • 出版日期2012-10-17