Automated lineshape analysis of complex NMR spectra for a novel synthetic tetrafluorobisphosphonate, a potential ligand for phosphoglycerate kinase

作者：Blackburn G M^*; Haegele G; Hottgenroth A; Ivory A J; Jakeman D L; Spiske R

来源：Phosphorus, Sulfur, and Silicon and the Related Elements, 2016, 191(3): 367-372.

DOI：10.1080/10426507.2015.1073281

• NMR
• Tetraalkyl 1,1,3,3-tetrafluoro-2,2-dihydroxypropane-1,3-bisphosphonates
• synthesis

Tetraalkyl 1,1,3,3-tetrafluoro-2,2-dihydroxypropane-1,3-bisphosphonates were prepared. The complex P-31{H-1}- and F-19-NMR spectra were analyzed as [[A](2)X](2) and related systems. Modern methods of automated spectral analysis using DAISY under WIN-NMR were applied.

• 出版日期2016-3-3