A convenient, high-sensitivity approach to multiple-resonance NMR at nanolitre volumes with inductively-coupled micro-coils

作者：Aguiar Pedro M; Jacquinot Jacques Francois; Sakellariou Dimitris^*

来源：Chemical Communications, 2011, 47(7): 2119-2121.

DOI：10.1039/c0cc04607h

We propose using singly-tuned mu-coils and H-1-detection to obtain high-sensitivity in lieu of miniaturizing cumbersome multi-resonance circuits, with the existing MAS probe circuitry/coil providing RF at other frequencies. We demonstrate two key building blocks in solid-state NMR: cross-polarization and heteronuclear decoupling. As well, a H-1-detected 2D HMQC is obtained.

• 出版日期2011
• 单位中国地震局