Dissipation and Residue Determination of Fluoroglycofen-Ethyl in Soybean and Soil by UPLC-MS-MS

作者：Geng Yue; Jia Ran; Li Chongjiu; Ma Xiaodong; Lin Yan^*

来源：Bulletin of Environmental Contamination and Toxicology, 2012, 89(3): 669-673.

DOI：10.1007/s00128-012-0681-0

• Fluoroglycofen-ethyl
• Dissipation
• Soybean
• Soil

A rapid, highly selective, and sensitive method was developed for detecting fluoroglycofen-ethyl in soybean seed, plant, and soil using UPLC-MS-MS. The detection limits of fluoroglycofen-ethyl in soybean seed, plant, and soil were 0.5, 1, and 1 mu g kg(-1), respectively. Recoveries ranged from 83.4 % to 99.2 %, in which intra-day RSDs were from 1.3 % to 6.7 % and inter-day RSDs were from 1.9 % to 7.0%. In the dissipation study, the half-lives of fluoroglycofen-ethyl were 34.8 (Shanxi) and 48.5 h (Heilongjiang) in soil and 43.3 h in soybean plant in both locations. The residues of fluoroglycofen-ethyl in all samples were below LODs 30 days before and during harvest.

• 出版日期2012-9
• 单位中国农业大学