Accounting for low-frequency synchrotron X-ray beam position fluctuations for dynamic visualizations

作者：Hinebaugh J; Challa P R; Bazylak A^*

来源：Journal of Synchrotron Radiation, 2012, 19: 994-1000.

DOI：10.1107/S0909049512039118

• synchrotron radiography
• fluctuations
• beam movement
• fuel cells
• polymer electrolyte membrane fuel cells
• 05B1-1 beamline

Synchrotron X-ray radiography on beamline 05B1-1 at the Canadian Light Source Inc. was employed to study dynamic liquid water transport in the porous electrode materials of polymer electrolyte membrane fuel cells. Dynamic liquid water distributions were quantified for each radiograph in a sequence, and non-physical liquid water measurements were obtained. It was determined that the position of the beam oscillated vertically with an amplitude of similar to 25 mu m at the sample and a frequency of similar to 50 mHz. In addition, the mean beam position moved linearly in the vertical direction at a rate of 0.74 mu m s(-1). No evidence of horizontal oscillations was detected. In this work a technique is presented to account for the temporal and spatial dependence of synchrotron beam intensity, which resulted in a significant reduction in false water thickness. This work provides valuable insight into the treatment of radiographic time-series for capturing dynamic processes from synchrotron radiation.

• 出版日期2012-11