A study on the consecutive preparation of silica powders and active carbon from rice husk ash

作者：An Dongmin; Guo Yupeng; Zou Bo; Zhu Yanchao; Wang Zichen^*

来源：Biomass and Bioenergy, 2011, 35(3): 1227-1234.

DOI：10.1016/j.biombioe.2010.12.014

• Rice husk ash
• Silica powders
• Active carbon
• Consecutive preparation
• Morphological feature

Rice husk ash (RHA) is an abundant agricultural by-product. The present research work deals with the production of silica powders and active carbon from RHA with a consecutive method. The RHA is firstly treated with acid leaching to remove mineral composition, and then is boiled with base to leach silica. The filtrate is used to synthesize silica powders with CO(2) precipitator and solid residue is used to prepare active carbon. The optimum conditions of preparing silica powders are as follows: the concentration of Na(2)CO(3) is 25 wt.%, the base-leached time is 4 h, and the impregnation ratio of Na(2)CO(3) solution to RHA is 6:1. The yield of silica leached from RHA is 84.57 wt.%. The synthesized silica powders are hydrated with amorphous structure, moreover, with a relative smooth surface and high purity. The residue is activated with potassium hydroxide (KOH) after base-leached. The activated carbons are found to be a mixture of micropore and mesopore pore structures. The maximum pore volume, BET surface area and iodine adsorption capacity of as-prepared active carbon can reach 1.22 cm(3)/g, 1936.62 m(2)/g and 1259.06 mg/g, respectively. Field emission scanning electron microscopy (SEM) is used to characterize the morphological features of the ash after step by step treatment.

• 出版日期2011-3
• 单位吉林大学