Development of an Integrated Thermocouple for the Accurate Sample Temperature Measurement During High Temperature Environmental Scanning Electron Microscopy (HT-ESEM) Experiments

作者：Podor Renaud^*; Pailhon Damien; Ravaux Johann; Brau Henri Pierre

来源：Microscopy and Microanalysis, 2015, 21(2): 307-312.

DOI：10.1017/S1431927615000252

• temperature
• ESEM
• calibration
• TC
• furnace

We have developed two integrated thermocouple (TC) crucible systems that allow precise measurement of sample temperature when using a furnace associated with an environmental scanning electron microscope (ESEM). Sample temperatures measured with these systems are precise (+/- 5 degrees C) and reliable. The TC crucible systems allow working with solids and liquids (silicate melts or ionic liquids), independent of the gas composition and pressure. These sample holder designs will allow end users to perform experiments at high temperature in the ESEM chamber with high precision control of the sample temperature.

• 出版日期2015-4
• 单位中国地震局