Design of an in-house ambient pressure AP-XPS using a bench-top X-ray source and the surface chemistry of ceria under reaction conditions

作者：Tao Franklin^*

来源：Chemical communications, 2012, 48(32): 3812-3814.

DOI：10.1039/c2cc17715c

A newin-house ambient pressure XPS (AP-XPS) was designed for the study of surfaces of materials under reaction conditions and during catalysis. Unique features of this in-house AP-XPS are the use of monochromated Al K alpha and integration of a minimized reaction cell, and working conditions of up to 500 degrees C in gases of tens of Torr. Generation of oxygen vacancies on ceria and filling them with oxygen atoms were characterized in operando.

• 出版日期2012