A light-through-side cell and co-used furnace designed for micro-Raman spectra study on volatile melts

作者：Hu Xian Wei^*; Li Huan; Gao Bing Liang; Liu Jing Jing; Shi Zhong Ning; Yu Jiang Yu; Wang Zhao Wen

来源：Chinese Chemical Letters, 2012, 23(11): 1291-1294.

DOI：10.1016/j.cclet.2012.10.004

• Light-through-side cell
• Raman spectroscopy
• Volatile melts
• Corner microlens
• Cell-around-heating body furnace

A new type of sample cell specially designed for micro-Raman spectra study on volatile melts is described. The cell is made of quartz. The lower section of the cell is circular ring-shaped and the one-end-closed hole in the cell is used for locating the heating body. The tube attached to the cell lid for placing the thermal couple is inserted into the sample, which ensures that the temperature measurement accuracy is good. The cell can be sealed for reducing the effect of the composition change caused by the inhomogeneous volatilization. During the Raman spectra scanning, the laser beam is transmitted into the cell through the side but not the top. Meanwhile, a furnace has been designed to match the cell. The heating body is closely coupled with the sample cell, and there is a hole on the side wall of the furnace for the entrance of the microlens. The assembly has performed well in the tested Raman spectrum measurement of molten NaNO3 at 602 degrees C.

• 出版日期2012-11
• 单位东北大学