Microstructural evolution of gas atomized Al-Zn-Mg-Cu-Zr powders during semi-solid rolling process

作者:Li, Feng-xian*; Liu, Yun-zhong; Yi, Jian-hong
来源:Transactions of Nonferrous Metals Society of China, 2014, 24(8): 2475-2481.
DOI:10.1016/S1003-6326(14)63373-2

摘要

Under H-2 atmosphere, the green strips were prepared from Al-5.8Zn-1.63Mg-2.22Cu-0.12Zr (mass fraction, %) powders by the semi-solid rolling process with a relative density from 76.1% to 88.0%. The role of temperature on microstructure and mechanical properties was investigated. With increasing rolling temperature from 580 to 610 degrees C, the disappearance of primary powder boundary and isolated pores, inter-diffusion of species and the change of grain boundary were accelerated. Moreover, the mechanism of microstructure evolution changes from the densification dominant regime to the coarsening dominant regime; the amount of eta (MgZn2) phase decreased and more Al2Cu particles precipitated at grain boundaries. The optimum temperature for semi-solid rolling of Al-5.8Zn-1.63Mg-2.22Cu-0.12Zr powders was determined. The liquid fraction in the range of 53% to 67% corresponds with a high density level of green strips. The present experimental analysis suggests that semi-solid powder rolling can be optimized to manufacture strips with high mechanical properties.