Microwave-assisted synthesis of thioamides with elemental sulfur

作者：Milen Matyas; Abranyi Balogh Peter; Dancso Andras; Keglevich Gyorgy^*

来源：Journal of Sulfur Chemistry, 2012, 33(1): 33-41.

DOI：10.1080/17415993.2011.640329

• benzylamines
• thionation
• thioamides
• fused piperidine derivatives
• microwave irradiation

Thioamides are prepared in moderate-to-good yields from the benzylamines or benzylamine derivatives by treatment with elemental sulfur under microwave and solvent-free conditions at 170 degrees C in 15 min. %26lt;br%26gt;[GRAPHICS] %26lt;br%26gt;.

• 出版日期2012