Determination of N, N-Dimethylformamide (DMF) in Waterborne Polyurethane by High Performance Liquid Chromatography

作者：Ren Keshuai; Sang Jun; Yu Lingyun; Wang Chunhua; Wu Mengru; Lin Wei^*

来源：Journal of the Society of Leather Technologists and Chemists, 2016, 100(4): 186-189.

A simple and sensitive method using high performance liquid chromatography (HPLC) has been developed for the determination of DMF in waterborne polyurethane (WPU) which is used in leather processing. Extraction of DMF is carried out by mechanical oscillation at room temperature for 10 minutes with water as the extraction solvent. Under optimal conditions, the limit of detection is 0.25mg L-1 and the recoveries are 95.2%similar to 102.1%. The proposed method has been successfully applied to the determination of DMF in different WPU samples.

• 出版日期2016-7
• 单位中国皮革和制鞋工业研究院; 四川大学