Deep eutectic solvent-based microwave-assisted extraction of genistin, genistein and apigenin from pigeon pea roots

作者：Cui, Qi; Peng, Xiao; Yao, Xiao-Hui; Wei, Zuo-Fu; Luo, Meng; Wang, Wei; Zhao, Chun-Jian; Fu, Yu-Jie^*; Zu, Yuan-Gang

来源：Separation and Purification Technology, 2015, 150: 63-72.

DOI：10.1016/j.seppur.2015.06.026

• Deep eutectic solvent
• Microwave-assisted extraction
• Pigeon pea roots
• Kinetics
• Response surface methodology

The purpose of the study was to develop a new deep eutectic solvent-based microwave-assisted extraction (DES-MAE) method for extracting the three major active compounds genistin, genistein and apigenin from pigeon pea roots. Optimal conditions for DES-MAE, proposed by the single factor and the Box-Behnken design (BBD) tests, were 30% of water in 1,6-hexanediol/ChCl (7:1, mol/mol) as the extraction solvent, microwave power 600W, liquid/solid ratio 14 mL/g, temperature 80 degrees C and time 11 min. The yields of genistin, genistein and apigenin reached 0.449, 0.617 and 0.221 mg/g DW, respectively. The kinetics experiment showed the prominent advantages of DES-MAE such as higher extraction efficiency than other extraction methods. The present results showed that DES could be a kind of green solvent for fast and efficient extraction of the active ingredients from plant materials.

• 出版日期2015-8-17
• 单位东北林业大学